葡萄中几种常用防治绿盲蝽农药的残留动态与风险评估

doi:10.3969/j.issn.1004-1524.2022.07.19

浙江农业学报 ›› 2022, Vol. 34 ›› Issue (7): 1513-1518.DOI: 10.3969/j.issn.1004-1524.2022.07.19

葡萄中几种常用防治绿盲蝽农药的残留动态与风险评估

孙淑媛¹(), 侯丽娜², 杨桂玲², 杜雨婷², 赵芸³^,^*()

1.长兴县农业农村局,浙江长兴 313100
2.浙江省农业科学院农产品质量安全与营养研究所,农业农村部农产品质量安全风险评估实验室,浙江杭州 310021
3.杭州市农业科学研究院,浙江杭州 310000

收稿日期:2020-09-08 出版日期:2022-07-25 发布日期:2022-07-26
通讯作者: 赵芸
作者简介:* 赵芸,E-mail: yunzhaohao@sina.com
孙淑媛(1988—),女,浙江长兴人,学士,工程师,从事农产品质量安全工作。E-mail: 334553381@qq.com
基金资助:
农产品质量安全标准化生产示范创建(“一县一品一策”)重大专项(ZJNY2020001);现代农业产业技术体系建设专项(CARS-29)

Residue dynamics and risk assessment of several pesticides commonly used for the control of Apolygus lucorum in grapes

SUN Shuyuan¹(), HOU Lina², YANG Guiling², DU Yuting², ZHAO Yun³^,^*()

1. Changxing Agriculture and Rural Affairs Bureau, Changxing 313100, Zhejiang, China
2. State Key Laboratory for Managing Biotic and Chemical Threats to the Quality and Safety of Agro-Products,Institute of Quality, Safety and Nutrition for Agricultural Products, Zhejiang Academy of Agricultural Sciences, Hangzhou 310021, China
3. Hangzhou Academy of Agricultural Sciences,Hangzhou 310000, China

Received:2020-09-08 Online:2022-07-25 Published:2022-07-26
Contact: ZHAO Yun

摘要/Abstract

摘要：

为探明葡萄中常用的几种防治绿盲蝽农药的残留规律和膳食风险,开展3种常用农药甲氨基阿维菌素苯甲酸盐(甲维盐)、噻虫嗪和啶虫脒在葡萄中的残留动态及膳食风险研究。结果表明,甲维盐、噻虫嗪、啶虫脒在葡萄中的降解均符合一级动力学方程,且使用14 d后均可降解至农药最高残留限量(MRL)值以下。3种农药在降解14 d的残留量的膳食风险评估结果表明,3种农药的慢性风险、急性风险和全膳食风险均小于100%,说明按照推荐的使用方法所选3种试验农药使用14 d后膳食风险较低,可以推荐用于绿盲蝽的防治,推荐安全间隔期为14 d。

关键词: 绿盲蝽, 甲维盐, 噻虫嗪, 啶虫脒, 残留动态, 膳食风险

Abstract:

To clarify the residues and dietary risks of several pesticides commonly used for the control of Apolygus lucorum in grapes, studies were carried out on three common pesticides: emamectinbenzoate, thiamethoxam and acetamiprid. The results showed that the degradation of these three pesticides in grape were in accordance with the first-order kinetic equation, and could degrade to below the maximum residue level (MRL) value after 14 days. Three kinds of pesticide residues in degradation of 14 days dietary risk assessment results showed that the three kinds of pesticide risk of chronic and acute risk and total dietary risk was less than 100%, which indicated that according to the recommended use method, the dietary risk of these three test pesticides was low after 14 days, and could be recommended for control Apolygus lucorum and the recommended security clearances was 14 days.

Key words: Apolygus lucorum, emamectin benzoate, thiamethoxam, acetamiprid, residual dynamics, risk assessment

中图分类号:

S663.1

孙淑媛, 侯丽娜, 杨桂玲, 杜雨婷, 赵芸. 葡萄中几种常用防治绿盲蝽农药的残留动态与风险评估[J]. 浙江农业学报, 2022, 34(7): 1513-1518.

SUN Shuyuan, HOU Lina, YANG Guiling, DU Yuting, ZHAO Yun. Residue dynamics and risk assessment of several pesticides commonly used for the control of Apolygus lucorum in grapes[J]. Acta Agriculturae Zhejiangensis, 2022, 34(7): 1513-1518.

图/表 4

参考文献 14

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消费量 Consumption	8~12岁儿童 Children aged 8 to 12	20~50岁成人 Adults aged 20 to 50
葡萄平均消费量Average grape consumption	4.87	5.21
人均葡萄的大份餐消费量Average consumption of large meals of grapes	366.72	570.29
水果平均消费量Average fruit consumption	141.50	151.50

消费量 Consumption	8~12岁儿童 Children aged 8 to 12	20~50岁成人 Adults aged 20 to 50
葡萄平均消费量Average grape consumption	4.87	5.21
人均葡萄的大份餐消费量Average consumption of large meals of grapes	366.72	570.29
水果平均消费量Average fruit consumption	141.50	151.50

农药 Pesticide	添加浓度 Addition concentration/(mg·kg^-1)	平均回收率 Average recovery/%	相对标准偏差 Relative standard deviation/%
甲维盐Emamectin benzoate	定量限Limit of quantitation(0.01)	85.0	7.1
	中Medium(0.05)	84.1	1.3
	高High(0.1)	85.8	0.8
噻虫嗪Thiamethoxam	定量限Limit of quantitation(0.01)	95.0	7.1
	中Medium (0.05)	115.6	4.4
	高High (0.1)	106.1	2.0
啶虫脒Acetamiprid	定量限Limit of quantitation(0.01)	87.5	3.5
	中Medium (0.05)	94.3	0.3
	高High (0.1)	85.8	4.7

农药 Pesticide	添加浓度 Addition concentration/(mg·kg^-1)	平均回收率 Average recovery/%	相对标准偏差 Relative standard deviation/%
甲维盐Emamectin benzoate	定量限Limit of quantitation(0.01)	85.0	7.1
	中Medium(0.05)	84.1	1.3
	高High(0.1)	85.8	0.8
噻虫嗪Thiamethoxam	定量限Limit of quantitation(0.01)	95.0	7.1
	中Medium (0.05)	115.6	4.4
	高High (0.1)	106.1	2.0
啶虫脒Acetamiprid	定量限Limit of quantitation(0.01)	87.5	3.5
	中Medium (0.05)	94.3	0.3
	高High (0.1)	85.8	4.7

农药名称 Pesticide	残留量 Residues/ (mg·kg^-1)	MRL/ (mg·kg^-1)	ADI/(mg· kg^-1·d^-1)	ARfD/(mg· kg^-1·d^-1)	慢性风险 Risk of chronic (%ADI)	急性风险 Risk of acute (%ARfD)	全膳食风险 Total dietary risk/%
甲维盐	0.000 2	0.03	0.000 5	—	0.001	—	32.57
Emamectin benzoate
噻虫嗪Thiamethoxam	0.066 5	0.5(浆果berry)	0.080 0	0.5	0.000 004	0.120	6.68
啶虫脒Acetamiprid	0.047 9	2	0.070 0	0.1	0.002	0.434	7.58

葡萄中几种常用防治绿盲蝽农药的残留动态与风险评估

Residue dynamics and risk assessment of several pesticides commonly used for the control of Apolygus lucorum in grapes

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