尿素包合法分离纯化山核桃油中亚油酸的研究

›› 2013, Vol. 25 ›› Issue (2): 0-353.

• 论文 •

尿素包合法分离纯化山核桃油中亚油酸的研究

陈丽敏1，2，郜海燕2，陈杭君2，*，房祥军2，穆宏磊2，刘大群2

1安徽农业大学茶与食品科技学院，安徽合肥230036；2浙江省农业科学院食品科学研究所，浙江杭州310021

收稿日期:1900-01-01 修回日期:1900-01-01 出版日期:2013-03-25 发布日期:2013-03-25

Study on the separation and purification of linoleic acid from Carya cathayensis Sarg. oil by urea adduction fractionation

CHEN Li-min;;GAO Hai-yan;CHEN Hang-jun;*;FANG Xiang-jun;MU Hong-lei;LIU Daqun

1College of Tea & Food Science and Technology， Anhui Agricultural University， Hefei 230036， China; 2Institute of Food Science， Zhejiang Academy of Agricultural Science， Hangzhou 310021， China

Received:1900-01-01 Revised:1900-01-01 Online:2013-03-25 Published:2013-03-25

摘要/Abstract

摘要： 为优化尿素包合纯化山核桃油中亚油酸的工艺，采用单因素和正交试验，研究了尿素包合反应中温度、时间、脂肪酸/尿素、甲醇/尿素等因素对亚油酸纯度及得率的影响。结果表明：在m（脂肪酸）/m（尿素）为0.3，V（甲醇）/m（尿素）为2.5，包合温度为-5℃，包合时间为24 h的优化条件下，山核桃油中亚油酸的含量由23.80%提高到80.73%。

关键词: 山核桃油, 尿素包合, 亚油酸

Abstract: Both single factor and orthogonal experiments were used to optimize conditions for purification of linoleic acid from Carya cathayensis Sarg. oil by urea adduction fractionation. Effects of adduction temperature， time， the ratio of fatty acid and urea and the ratio of methanol and urea on the purity and yield of linoleic acid were investigated. The results showed that the optimal purification conditions were the ratio of fatty acid and urea （m/m） at 0.3， the ratio of methanol and urea （V/m） at 2.5， adduction temperature at -5℃， and adduction time of 24 h, in which content of linoleic acid in Carya cathayensis Sarg. oil increased from 23.80% to 80.73%.

Key words: Carya cathayensis Sarg. oil, urea adduction fractionation, linoleic acid

陈丽敏;郜海燕;陈杭君;*;房祥军;穆宏磊;刘大群. 尿素包合法分离纯化山核桃油中亚油酸的研究[J]. , 2013, 25(2): 0-353.

CHEN Li-min;GAO Hai-yan;CHEN Hang-jun;*;FANG Xiang-jun;MU Hong-lei;LIU Daqun. Study on the separation and purification of linoleic acid from Carya cathayensis Sarg. oil by urea adduction fractionation[J]. , 2013, 25(2): 0-353.

尿素包合法分离纯化山核桃油中亚油酸的研究

Study on the separation and purification of linoleic acid from Carya cathayensis Sarg. oil by urea adduction fractionation

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