Acta Agriculturae Zhejiangensis ›› 2023, Vol. 35 ›› Issue (5): 1168-1177.DOI: 10.3969/j.issn.1004-1524.2023.05.21
• Quality and Safety of Agricultural Products • Previous Articles Next Articles
WANG Xiaoyan1,2(
), HAN Yanchao2, WU Weijie2, DENG Shanggui1, CHEN Hangjun2, FANG Xiangjun2, GAO Haiyan2,*(
)
Received:2022-02-28
Online:2023-05-25
Published:2023-06-01
CLC Number:
WANG Xiaoyan, HAN Yanchao, WU Weijie, DENG Shanggui, CHEN Hangjun, FANG Xiangjun, GAO Haiyan. Effects of different drying methods on quality and volatile flavor of pineapple[J]. Acta Agriculturae Zhejiangensis, 2023, 35(5): 1168-1177.
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URL: http://www.zjnyxb.cn/EN/10.3969/j.issn.1004-1524.2023.05.21
| 项目 Project | 评分标准 Scoring criteria | 感官评分 Sensory score |
|---|---|---|
| 外观Appearance | 组织饱满,透亮,有光泽The tissue is full, transparent and shiny | 16~20 |
| 组织略有萎缩,微透亮,有光泽The tissue is slightly atrophic, slightly transparent and shiny | 11~15 | |
| 组织干缩严重,无透明光泽The tissue shrinks seriously and has no transparent luster | 5~10 | |
| 色泽Color | 色泽金黄 Golden color | 16~20 |
| 暗黄色 Dark yellow | 11~15 | |
| 黑褐色 Dark brown | 5~10 | |
| 风味Flavor | 酸甜适中 Moderate sour and sweet | 26~30 |
| 偏酸或偏甜 Sour or sweet | 16~25 | |
| 苦涩有异味 Bitter and astringent with peculiar smell | 5~15 | |
| 口感Taste | 有韧性,软硬适中 It has toughness and moderate hardness | 26~30 |
| 干硬 Dry hard | 16~25 | |
| 无韧性 No toughness | 5~15 |
Table 1 Sensory scoring criteria
| 项目 Project | 评分标准 Scoring criteria | 感官评分 Sensory score |
|---|---|---|
| 外观Appearance | 组织饱满,透亮,有光泽The tissue is full, transparent and shiny | 16~20 |
| 组织略有萎缩,微透亮,有光泽The tissue is slightly atrophic, slightly transparent and shiny | 11~15 | |
| 组织干缩严重,无透明光泽The tissue shrinks seriously and has no transparent luster | 5~10 | |
| 色泽Color | 色泽金黄 Golden color | 16~20 |
| 暗黄色 Dark yellow | 11~15 | |
| 黑褐色 Dark brown | 5~10 | |
| 风味Flavor | 酸甜适中 Moderate sour and sweet | 26~30 |
| 偏酸或偏甜 Sour or sweet | 16~25 | |
| 苦涩有异味 Bitter and astringent with peculiar smell | 5~15 | |
| 口感Taste | 有韧性,软硬适中 It has toughness and moderate hardness | 26~30 |
| 干硬 Dry hard | 16~25 | |
| 无韧性 No toughness | 5~15 |
| 处理 Treatment | 外观Appearance | 色泽Color | 风味Flavor | 口感Taste | 总分Total score |
|---|---|---|---|---|---|
| T1 | 12±1 b | 15±1 b | 17±3 b | 25±1 b | 69±3 c |
| T2 | 16±2 a | 19±1 a | 24±2 a | 27±1 a | 86±4 a |
| T3 | 15±1 a | 18±1 a | 23±3 a | 24±2 b | 80±4 b |
Table 2 Effects of different drying methods on sensory score of pineapple
| 处理 Treatment | 外观Appearance | 色泽Color | 风味Flavor | 口感Taste | 总分Total score |
|---|---|---|---|---|---|
| T1 | 12±1 b | 15±1 b | 17±3 b | 25±1 b | 69±3 c |
| T2 | 16±2 a | 19±1 a | 24±2 a | 27±1 a | 86±4 a |
| T3 | 15±1 a | 18±1 a | 23±3 a | 24±2 b | 80±4 b |
| 处理Treatment | L* | a* | b* | ΔE |
|---|---|---|---|---|
| T1 | 60.17±2.31 c | 5.14±1.79 a | 46.16±1.84 a | 58.06±1.80 a |
| T2 | 76.46±1.81 b | -3.95±1.28 b | 44.61±2.00 a | 47.40±1.94 b |
| T3 | 92.33±0.64 a | -5.75±0.32 c | 27.06±0.98 b | 26.33±0.69 c |
Table 3 Effects of different drying methods on color of pineapple
| 处理Treatment | L* | a* | b* | ΔE |
|---|---|---|---|---|
| T1 | 60.17±2.31 c | 5.14±1.79 a | 46.16±1.84 a | 58.06±1.80 a |
| T2 | 76.46±1.81 b | -3.95±1.28 b | 44.61±2.00 a | 47.40±1.94 b |
| T3 | 92.33±0.64 a | -5.75±0.32 c | 27.06±0.98 b | 26.33±0.69 c |
| 处理Treatment | 硬度Hardness/g | 弹性Springiness | 内聚性Cohesiveness | 咀嚼性Chewiness | 回复性Resilience |
|---|---|---|---|---|---|
| T1 | 260.22±54.57 b | 0.87±0.12 a | 0.55±0.13 b | 133.90±19.44 b | 0.09±0.02 c |
| T2 | 227.44±89.77 b | 0.92±0.07 a | 0.72±0.11 a | 128.87±46.40 b | 0.24±0.02 a |
| T3 | 722.23±142.42 a | 0.69±0.14 b | 0.56±0.03 b | 256.77±16.57 a | 0.17±0.03 b |
Table 4 Effects of different drying methods on texturer of pineapple
| 处理Treatment | 硬度Hardness/g | 弹性Springiness | 内聚性Cohesiveness | 咀嚼性Chewiness | 回复性Resilience |
|---|---|---|---|---|---|
| T1 | 260.22±54.57 b | 0.87±0.12 a | 0.55±0.13 b | 133.90±19.44 b | 0.09±0.02 c |
| T2 | 227.44±89.77 b | 0.92±0.07 a | 0.72±0.11 a | 128.87±46.40 b | 0.24±0.02 a |
| T3 | 722.23±142.42 a | 0.69±0.14 b | 0.56±0.03 b | 256.77±16.57 a | 0.17±0.03 b |
Fig.1 Effects of different drying methods on contents of VC, total sugar, total phenol and soluble protein of pineapple Bars marked without the same letters indicate significant difference at P<0.05.
| 类别 Type | 风味物质 Flavor compounds | 不同处理下的含量Content under different treatments/(μg·kg-1) | 特征香味 Characteristic aroma | ||||||
|---|---|---|---|---|---|---|---|---|---|
| T1 | T2 | T3 | |||||||
| 酯类 | 乙酸甲酯Methyl acetate | ND | ND | 0.01 | 水果香Fruity aroma | ||||
| Esters | 乙酸乙酯Ethyl acetate | ND | 5.03 | ND | 水果香Fruity aroma | ||||
| 丁酸甲酯Methyl butyrate | ND | ND | 0.44 | 苹果香Apple aroma | |||||
| 2-甲基丁酸甲酯Methyl 2-methylbutyrate | ND | 2.32 | 2.68 | 水果香Fruity aroma | |||||
| 2-甲基丁酸乙酯Ethyl 2-methylbutyrate | ND | 12.65 | ND | 苹果香Apple aroma | |||||
| 乙酸异戊酯Isopentyl acetate | ND | 10.02 | ND | 香蕉香Banana aroma | |||||
| 当归内酯Alpha-angelicalactone | 4.48 | ND | ND | 巧克力香Chocolate aroma | |||||
| 丙二酸二甲酯Dimethyl malonate | 2.45 | 7.24 | 8.21 | — | |||||
| 己酸乙酯Ethyl caproate | 2.60 | 159.06 | 177.75 | 菠萝香Pineapple aroma | |||||
| 3-己烯酸乙酯Ethyl cis-3-hexenoate | ND | 15.29 | ND | 水果香Fruity aroma | |||||
| 庚酸甲酯Methyl enanthate | ND | 3.21 | 3.56 | — | |||||
| 3-甲硫基丙酸甲酯Methyl 3-methylthiopropionate | 4.11 | 19.05 | 21.06 | 稀释时有甜果香 | |||||
| Sweet fruity aroma when diluted | |||||||||
| 庚酸乙酯Ethyl heptanoate | ND | ND | 18.21 | 菠萝香Pineapple aroma | |||||
| 辛酸甲酯Methyl octanoate | 18.78 | 103.94 | 114.18 | 果香和酒香 Fruit and wine aroma | |||||
| 丙位己内酯γ-Hexalactone | 6.57 | 10.61 | 11.66 | 药草香、焦糖香 | |||||
| Herbal fragrance, caramelized fragrance | |||||||||
| 辛酸乙酯Ethyl caprylate | 8.91 | 20.43 | 632.46 | 水果香、菠萝香 | |||||
| Fruity aroma, pineapple aroma | |||||||||
| 苯乙酸甲酯Methyl phenylacetate | ND | ND | 1.44 | 蜂蜜香Honey fragrance | |||||
| 苯乙酸乙酯Ethyl phenylacetate | ND | 7.47 | ND | 蜂蜜香Honey fragrance | |||||
| 癸酸甲酯Methyl caprate | 4.81 | 6.29 | 6.83 | — | |||||
| 丙位十二内酯2(3H)-Furanone,dihydro-5-octyl- | ND | 0.83 | 0.89 | 水果香Fruity aroma | |||||
| 癸酸乙酯Ethyl caprate | ND | 100.25 | ND | 果香和酒香Fruit and wine aroma | |||||
| 邻苯二甲酸二甲酯Dimethyl phthalate | 1.44 | 4.33 | 4.69 | — | |||||
| 醇类 | 乙醇Ethanol | ND | 4.58 | ND | 芳香气味Aromatic odor | ||||
| Alcohols | 4-萜烯醇Terpinen-4-ol | ND | ND | 2.52 | 暖胡椒香Warm pepper aroma | ||||
| 酮类 | 4-羟基-2-丁酮4-Hydroxy-2-butanone | ND | ND | 5.78 | — | ||||
| Ketones | 甲基庚烯酮6-Methyl-5-hepten-2-one | 1.63 | 4.19 | 4.57 | 柠檬草香Lemongrass fragrance | ||||
| 呋喃酮Furaneol | ND | 7.54 | 5.90 | 水果香Fruity aroma | |||||
| 醛类 | 异戊醛Isovaleraldehyde | 2.02 | ND | ND | 苹果香Apple aroma | ||||
| Aldehyde | 2-甲基丁醛2-Methylbutyraldehyde | 1.76 | ND | ND | — | ||||
| 正己醛Caproaldehyde | 2.19 | 4.22 | 4.77 | 刺激性气味Pungent odor | |||||
| 糠醛2-Furaldehyde | 285.85 | 18.14 | ND | 杏仁气味Almond odor | |||||
| 庚醛Heptanal | 3.24 | 2.96 | 3.31 | 水果香Fruity aroma | |||||
| (E)-2-庚烯醛(E)-Hept-2-enal | ND | ND | 2.51 | 脂芳香Fatty aroma | |||||
| 苯甲醛Benzaldehyde | 6.17 | 3.36 | 3.64 | 苦杏仁味Bitter almond flavor | |||||
| 5-甲基呋喃醛5-Methylfurfural | 15.88 | ND | ND | 焦糖香Caramelized fragrance | |||||
| 正辛醛N-capryl(ic) aldehyde | ND | ND | 109.59 | 水果香Fruity aroma | |||||
| 苯乙醛Phenylacetaldehyde | 68.60 | 8.19 | ND | 稀释后甜果香 | |||||
| Sweet fruity aroma after dilution | |||||||||
| 壬醛Nonanal | 48.12 | 7.54 | 103.52 | 稀释时有玫瑰和柑橘香 | |||||
| Rose and citrus aromas when diluted | |||||||||
| 癸醛Decanal | 17.89 | 58.70 | 22.34 | 稀释时呈果香Fruit aroma when diluted | |||||
| 反式-2-癸烯醛Trans-2-decenal | 7.05 | 17.84 | 19.46 | — | |||||
| 2-十一烯醛2-Undecenal | ND | ND | 109.44 | 柑橘香Citrus aroma | |||||
| 烯烃类 | 环庚三烯Cycloheptatriene | 3.00 | ND | 2.87 | — | ||||
| Alkenes | (+)-柠檬烯(+)-Limonene | ND | 98.35 | ND | 柑橘香Citrus aroma | ||||
| 罗勒烯(Z)-β-ocimene | 13.35 | 15.76 | ND | 花香Fragrance of flower | |||||
| 1,3,5-十一碳三烯1,3,5-Undecatriene | 7.40 | 7.12 | 7.86 | 格蓬香Gepeng incense | |||||
| (-)-alpha-古芸烯(-)-alpha-Gurjunene | 26.00 | 62.23 | 67.72 | — | |||||
| β-石竹烯β-Caryophyllene | ND | 3.04 | ND | 丁香香味Clove aroma | |||||
| (+)-苜蓿烯Sativene | 13.74 | 46.92 | 51.14 | — | |||||
| 萜品油烯Terpinolene | ND | 3.16 | ND | 柠檬香Lemon aroma | |||||
| 佛术烯Eremophilene | 31.28 | 61.15 | 65.49 | — | |||||
| (-)-异喇叭烯(-)-Isoledene | 36.78 | 52.40 | 56.38 | — | |||||
| 酸类 | 乙酸Acetic acid | 1.33 | 0.43 | ND | 刺激性气味Pungent odor | ||||
| Acids | 正己酸1-Hexanoic acid | ND | 17.67 | ND | 刺激性气味Pungent odor | ||||
| 2-甲基丁酸2-Methylbutyric acid | ND | 0.63 | 0.70 | 低浓度时呈果香 | |||||
| Fruit aroma at low concentration | |||||||||
| 其他 | 乙苯Ethylbenzene | 2.05 | 1.81 | 2.04 | 芳香气味Aromatic odor | ||||
| Others | 间二甲苯m-Xylene | 4.53 | 0.99 | 1.14 | — | ||||
| 2-乙酰基呋喃2-Acetylfuran | 17.25 | 1.29 | ND | 焦糖香Caramelized fragrance | |||||
Table 5 Effects of different drying methods on volatile flavor compounds of pineapple
| 类别 Type | 风味物质 Flavor compounds | 不同处理下的含量Content under different treatments/(μg·kg-1) | 特征香味 Characteristic aroma | ||||||
|---|---|---|---|---|---|---|---|---|---|
| T1 | T2 | T3 | |||||||
| 酯类 | 乙酸甲酯Methyl acetate | ND | ND | 0.01 | 水果香Fruity aroma | ||||
| Esters | 乙酸乙酯Ethyl acetate | ND | 5.03 | ND | 水果香Fruity aroma | ||||
| 丁酸甲酯Methyl butyrate | ND | ND | 0.44 | 苹果香Apple aroma | |||||
| 2-甲基丁酸甲酯Methyl 2-methylbutyrate | ND | 2.32 | 2.68 | 水果香Fruity aroma | |||||
| 2-甲基丁酸乙酯Ethyl 2-methylbutyrate | ND | 12.65 | ND | 苹果香Apple aroma | |||||
| 乙酸异戊酯Isopentyl acetate | ND | 10.02 | ND | 香蕉香Banana aroma | |||||
| 当归内酯Alpha-angelicalactone | 4.48 | ND | ND | 巧克力香Chocolate aroma | |||||
| 丙二酸二甲酯Dimethyl malonate | 2.45 | 7.24 | 8.21 | — | |||||
| 己酸乙酯Ethyl caproate | 2.60 | 159.06 | 177.75 | 菠萝香Pineapple aroma | |||||
| 3-己烯酸乙酯Ethyl cis-3-hexenoate | ND | 15.29 | ND | 水果香Fruity aroma | |||||
| 庚酸甲酯Methyl enanthate | ND | 3.21 | 3.56 | — | |||||
| 3-甲硫基丙酸甲酯Methyl 3-methylthiopropionate | 4.11 | 19.05 | 21.06 | 稀释时有甜果香 | |||||
| Sweet fruity aroma when diluted | |||||||||
| 庚酸乙酯Ethyl heptanoate | ND | ND | 18.21 | 菠萝香Pineapple aroma | |||||
| 辛酸甲酯Methyl octanoate | 18.78 | 103.94 | 114.18 | 果香和酒香 Fruit and wine aroma | |||||
| 丙位己内酯γ-Hexalactone | 6.57 | 10.61 | 11.66 | 药草香、焦糖香 | |||||
| Herbal fragrance, caramelized fragrance | |||||||||
| 辛酸乙酯Ethyl caprylate | 8.91 | 20.43 | 632.46 | 水果香、菠萝香 | |||||
| Fruity aroma, pineapple aroma | |||||||||
| 苯乙酸甲酯Methyl phenylacetate | ND | ND | 1.44 | 蜂蜜香Honey fragrance | |||||
| 苯乙酸乙酯Ethyl phenylacetate | ND | 7.47 | ND | 蜂蜜香Honey fragrance | |||||
| 癸酸甲酯Methyl caprate | 4.81 | 6.29 | 6.83 | — | |||||
| 丙位十二内酯2(3H)-Furanone,dihydro-5-octyl- | ND | 0.83 | 0.89 | 水果香Fruity aroma | |||||
| 癸酸乙酯Ethyl caprate | ND | 100.25 | ND | 果香和酒香Fruit and wine aroma | |||||
| 邻苯二甲酸二甲酯Dimethyl phthalate | 1.44 | 4.33 | 4.69 | — | |||||
| 醇类 | 乙醇Ethanol | ND | 4.58 | ND | 芳香气味Aromatic odor | ||||
| Alcohols | 4-萜烯醇Terpinen-4-ol | ND | ND | 2.52 | 暖胡椒香Warm pepper aroma | ||||
| 酮类 | 4-羟基-2-丁酮4-Hydroxy-2-butanone | ND | ND | 5.78 | — | ||||
| Ketones | 甲基庚烯酮6-Methyl-5-hepten-2-one | 1.63 | 4.19 | 4.57 | 柠檬草香Lemongrass fragrance | ||||
| 呋喃酮Furaneol | ND | 7.54 | 5.90 | 水果香Fruity aroma | |||||
| 醛类 | 异戊醛Isovaleraldehyde | 2.02 | ND | ND | 苹果香Apple aroma | ||||
| Aldehyde | 2-甲基丁醛2-Methylbutyraldehyde | 1.76 | ND | ND | — | ||||
| 正己醛Caproaldehyde | 2.19 | 4.22 | 4.77 | 刺激性气味Pungent odor | |||||
| 糠醛2-Furaldehyde | 285.85 | 18.14 | ND | 杏仁气味Almond odor | |||||
| 庚醛Heptanal | 3.24 | 2.96 | 3.31 | 水果香Fruity aroma | |||||
| (E)-2-庚烯醛(E)-Hept-2-enal | ND | ND | 2.51 | 脂芳香Fatty aroma | |||||
| 苯甲醛Benzaldehyde | 6.17 | 3.36 | 3.64 | 苦杏仁味Bitter almond flavor | |||||
| 5-甲基呋喃醛5-Methylfurfural | 15.88 | ND | ND | 焦糖香Caramelized fragrance | |||||
| 正辛醛N-capryl(ic) aldehyde | ND | ND | 109.59 | 水果香Fruity aroma | |||||
| 苯乙醛Phenylacetaldehyde | 68.60 | 8.19 | ND | 稀释后甜果香 | |||||
| Sweet fruity aroma after dilution | |||||||||
| 壬醛Nonanal | 48.12 | 7.54 | 103.52 | 稀释时有玫瑰和柑橘香 | |||||
| Rose and citrus aromas when diluted | |||||||||
| 癸醛Decanal | 17.89 | 58.70 | 22.34 | 稀释时呈果香Fruit aroma when diluted | |||||
| 反式-2-癸烯醛Trans-2-decenal | 7.05 | 17.84 | 19.46 | — | |||||
| 2-十一烯醛2-Undecenal | ND | ND | 109.44 | 柑橘香Citrus aroma | |||||
| 烯烃类 | 环庚三烯Cycloheptatriene | 3.00 | ND | 2.87 | — | ||||
| Alkenes | (+)-柠檬烯(+)-Limonene | ND | 98.35 | ND | 柑橘香Citrus aroma | ||||
| 罗勒烯(Z)-β-ocimene | 13.35 | 15.76 | ND | 花香Fragrance of flower | |||||
| 1,3,5-十一碳三烯1,3,5-Undecatriene | 7.40 | 7.12 | 7.86 | 格蓬香Gepeng incense | |||||
| (-)-alpha-古芸烯(-)-alpha-Gurjunene | 26.00 | 62.23 | 67.72 | — | |||||
| β-石竹烯β-Caryophyllene | ND | 3.04 | ND | 丁香香味Clove aroma | |||||
| (+)-苜蓿烯Sativene | 13.74 | 46.92 | 51.14 | — | |||||
| 萜品油烯Terpinolene | ND | 3.16 | ND | 柠檬香Lemon aroma | |||||
| 佛术烯Eremophilene | 31.28 | 61.15 | 65.49 | — | |||||
| (-)-异喇叭烯(-)-Isoledene | 36.78 | 52.40 | 56.38 | — | |||||
| 酸类 | 乙酸Acetic acid | 1.33 | 0.43 | ND | 刺激性气味Pungent odor | ||||
| Acids | 正己酸1-Hexanoic acid | ND | 17.67 | ND | 刺激性气味Pungent odor | ||||
| 2-甲基丁酸2-Methylbutyric acid | ND | 0.63 | 0.70 | 低浓度时呈果香 | |||||
| Fruit aroma at low concentration | |||||||||
| 其他 | 乙苯Ethylbenzene | 2.05 | 1.81 | 2.04 | 芳香气味Aromatic odor | ||||
| Others | 间二甲苯m-Xylene | 4.53 | 0.99 | 1.14 | — | ||||
| 2-乙酰基呋喃2-Acetylfuran | 17.25 | 1.29 | ND | 焦糖香Caramelized fragrance | |||||
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