不同提取方法所得山茶油的品质比较

doi:10.3969/j.issn.1004-1524.2017.07.19

浙江农业学报 ›› 2017, Vol. 29 ›› Issue (7): 1195-1200.DOI: 10.3969/j.issn.1004-1524.2017.07.19

不同提取方法所得山茶油的品质比较

葛杭丽¹, 彭丽¹, 孟祥河¹, 肖朝耿^{1, 2, *}

1.浙江工业大学海洋学院,浙江杭州 310000;
2.浙江省农业科学院食品科学研究所,浙江杭州 310021

收稿日期:2017-02-23 出版日期:2017-07-20 发布日期:2017-07-24
通讯作者: 肖朝耿,E-mail:xiaochaogeng@163.com
作者简介:葛杭丽(1991—),女,浙江杭州人,硕士研究生,研究方向为粮食油脂与植物蛋白。E-mail:ghl1817@163.com

Comparison into quality of Camellia oil extracted by different methods

GE Hangli¹, PENG Li¹, MENG Xianghe¹, XIAO Chaogeng^{1, 2, *}

1. Ocean College, Zhejiang University of Technology, Hangzhou 310000, China;
2. Institute of Food Processing, Zhejiang Academy of Agricultural Sciences, Hangzhou 310021, China

Received:2017-02-23 Online:2017-07-20 Published:2017-07-24

摘要/Abstract

摘要： 采用化学分析法、HPLC、GC-MS法分析水酶法、水代溶剂法、有机溶剂萃取法所得山茶油的理化指标、角鲨烯、维生素E、主要脂肪酸含量及组成。结果显示,水酶法和水代溶剂法提取山茶油的感官指标和理化指标相近,优于有机溶剂萃取法所提山茶油。水酶法所提山茶油中的角鲨烯(255.00 μg·g^-1)、α-维生素E(247.44 μg·g^-1)、β-维生素E(46.05 μg·g^-1)、δ-维生素E(11.65 μg·g^-1)含量高于其他2种方法所提山茶油。各方法提取的山茶油中脂肪酸组成没有显著性差异。从感官、理化指标和特征活性物质角鲨烯及维生素E含量综合来看,水酶法提取山茶油的品质较优,在工业生产中具有较大的应用前景。

关键词: 提取方法, 水酶法, 山茶油, 品质

Abstract: In order to compare and analyze the quality of Camellia oil extracted by aqueous enzymatic extraction, aqueous extraction and organic solvent extraction, physicochemical indexes of extracted lipids were analyzed, as squalene and vitamin E (V_E) contents, and fatty acid composition were determined by chemical analysis, HPLC and GC-MS methods. It was shown that the sensory and physicochemical index of Camellia oil extracted by aqueous enzymatic extraction and aqueous extraction was similar, and was better than that extracted by organic solvent. The contents of squalene and α-,β-,δ-V_E in Camellia oil extracted by aqueous enzymatic extraction were 255.00, 247.44, 46.05, 11.65 μg·g^-1, respectively, and were higher than those extracted by other methods. In general, aqueous enzymatic method was superior for Camellia oil extraction to other methods in term of sensory quality, physicochemical index as well as the content of functional material (squalene and V_E), and thus possessed greater potential for industrial implication.

Key words: extraction method, aqueous enzymatic method, Camellia oil, quality

中图分类号:

葛杭丽, 彭丽, 孟祥河, 肖朝耿. 不同提取方法所得山茶油的品质比较[J]. 浙江农业学报, 2017, 29(7): 1195-1200.

GE Hangli, PENG Li, MENG Xianghe, XIAO Chaogeng. Comparison into quality of Camellia oil extracted by different methods[J]. , 2017, 29(7): 1195-1200.

参考文献

[1] 吴万春. 植物学[M]. 广州: 华南理工大学出版社, 2002: 278.
[2] 方学智, 姚小华, 王开良, 等. 不同制油方法对油茶籽油品质的影响[J]. 中国油脂, 2009, 34(1):23-26.
FANG X Z, YAO X H, WANG K L, et al. Effects of extraction methods on the quality of oil-tea camellia seed oil[J]. China Oils and Fats , 2009, 34(1): 23-26. (in Chinese with English abstract)
[3] 龙正海, 王道平. 油茶籽油与橄榄油化学成分研究[J]. 中国粮油学报, 2008, 23(2):121-123.
LONG Z H, WANG D P. Chemical constituents of olive oil and from Camellia oleifera seed oil[J]. Journal of the Chinese Cereals and Oils Association , 2008, 23(2): 121-123. (in Chinese with English abstract)
[4] TENLLADO D, REGLERO G, TORRES C F. A combined procedure of supercritical fluid extraction and molecular distillation for the purification of alkylglycerols from shark liver oil[J]. Separation & Purification Technology , 2011, 83(22):74-81.
[5] 刘朝霞, 陈海光, 刘丽微. 山茶油提取方法研究进展[J]. 安徽农业科学, 2011, 39(10):6067-6069.
LIU Z X, CHEN H G, LIU L W. Research progress in extraction of camellia oil[J]. Journal of Anhui Agricultural Sciences , 2011, 39(10): 6067-6069. (in Chinese with English abstract)
[6] 孟维, 李湘洲, 吴志平, 等. 茶籽油提取工艺的实验研究[J]. 食品科技, 2010, 35(4):153-155.
MENG W, LI X Z, WU Z P, et al. Experimental study on extraction of camellia seed oil[J]. Food Science and Technology , 2010, 35(4): 153-155. (in Chinese with English abstract)
[7] YU X, LI Q, DU S, et al. A novel process for the aqueous extraction of oil from Camellia oleifera seeds and its antioxidant activity[J]. Grasas Y Aceites , 2013, 64(4): 407-414.
[8] FANG X, FEI X, SUN H, et al. Aqueous enzymatic extraction and demulsification of camellia seed oil ( Camellia oleifera Abel.) and the oil's physicochemical properties[J]. European Journal of Lipid Science & Technology , 2015, 118(2):244-251.
[9] 何伟. 反相液相色谱法测定植物油中VE含量的方法研究[D]. 长沙:湖南农业大学, 2011.
HE W. Study on determination of vitamin e in vegetable oil by reversed-phase liquid chromatography[D]. Changsha: Hunan Agricultural University, 2011.(in Chinese with English abstract)
[10] 杨辉. 茶油提取新工艺及其品质的研究[D]. 南昌:南昌大学, 2012.
YANG H. Study on new extraction processes and quality of camellia oil[D]. Nanchang: Nanchang University, 2012. (in Chinese with English abstract)
[11] ZHANG S, ZU Y, FU Y, et al. Supercritical carbon dioxide extraction of seed oil from yellow horn ( Xanthoceras sorbifolia Bunge.) and its anti-oxidant activity[J]. Bioresource Technology , 2010, 101(7):2537-2544.
[12] 甘秀海, 梁志远, 赵超, 等. 油茶籽油和茶籽油的提取及其品质特性[J]. 贵州农业科学, 2015, 43(9):181-185.
GAN X H, LIANG Z Y, ZHAO C, et al. Extractions and quality characteristics of Camellia oleifera oil and Camellia sinensis oil[J]. Guizhou Agricultural Sciences , 2015, 43(9): 181-185. (in Chinese with English abstract)
[13] 鲍会梅. 色拉油中过氧化值含量测定方法的研究[J]. 粮油加工, 2010(5):12-15.
BAO H M. Study on determination method of peroxide value in salad oil[J]. Cereals and Oils Processing , 2010(5):12-15.(in Chinese)
[14] 章绍兵, 王璋. 水酶法从菜籽中提取油及水解蛋白的研究[J]. 农业工程学报, 2007, 23(9):213-219.
ZHANG S B, WANG Z. Aqueous enzymatic extraction technology of oil and protein hydrolysates from rapeseed[J]. Transactions of the Chinese Society of Agricultural Engineering , 2007, 23(9): 213-219. (in Chinese with English abstract)
[15] 方学智. 油茶籽油脂构成、变化规律和水酶法制取工艺研究[D]. 杭州:浙江大学, 2015.
FANG X Z. Study on lipid composition and variation of camellia oil and aqueous enzymatic extraction[D]. Hangzhou: Zhejiang University, 2015. (in Chinese with English abstract)
[16] FRUHWIRTH G O, WENZL T, EL-TOUKHY R, et al. Fluorescence screening of antioxidant capacity in pumpkin seed oils and other natural oils[J]. European Journal of Lipid Science & Technology , 2003, 105: 266-274.
[17] JIAO J, LI Z G, GAI Q Y, et al. Microwave-assisted aqueous enzymatic extraction of oil from pumpkin seeds and evaluation of its physicochemical properties, fatty acid compositions and antioxidant activities[J]. Food Chemistry , 2014, 147(6):17-24.
[18] 张菁菁, 沈根明, 华国浩, 等. 高温应激下添加维生素E对蛋鸡血液生化指标和产蛋性能的影响[J]. 浙江农业学报, 2016, 28(2):228-233.
ZHANG J J, SHEN G M, HUA G H, et al. Effect of vitamin E on blood biochemical index and laying performance in laying hens under heat stress[J]. Acta Agriculturae Zhejiangensis , 2016, 28(2): 228-233. (in Chinese with English abstract)
[19] DIRAMAN H, DİBEKLİOĞLU H. Characterization of Turkish virgin olive oils produced from early harvest olives[J]. Journal of the American Oil Chemists' Society , 2009, 86(7):663-674.
[20] BABOLI Z M, KORDI A A S. Characteristics and composition of watermelon seed oil and solvent extraction parameters effects[J]. Journal of the American Oil Chemists' Society , 2010, 87(6):667-671.
[21] PRANABENDU M, HOSAHALLIS R, CHANG K S. Pumpkin ( Cucurbita maxima ) seed oil extraction using supercritical carbon dioxide and physicochemical properties of the oil[J]. Journal of Food Engineering , 2009, 95(1):208-213.
[22] 姜慧仙. 水酶法提取油茶籽油的工艺及品质研究[D]. 上海:上海师范大学, 2013.
JIANG H X. Study on aqueous enzymatic extraction processes and quality of camellia oil[D]. Shanghai: Shanghai Normal University, 2013. (in Chinese with English abstract)

不同提取方法所得山茶油的品质比较

Comparison into quality of Camellia oil extracted by different methods

RichHTML

PDF (PC)

可视化

被引次数

摘要/Abstract

引用本文

使用本文

参考文献

相关文章 15

编辑推荐

Metrics

本文评价

[1]	温明霞, 张顺昌, 吴韶辉, 胡丽鹏, 王鹏, 黄贝. 蛋白水解氨基酸肥料对红美人杂柑果实品质的影响[J]. 浙江农业学报, 2021, 33(3): 422-428.
[2]	陈丹, 汤翠凤, 董超, 甘树仙, 李俊, 阿新祥, 张斐斐, 杨雅云, 牛赛赛, 戴陆园. 云南软米地方品种籽粒淀粉品质特性研究[J]. 浙江农业学报, 2021, 33(2): 203-214.
[3]	李甜竹, 孙玉文, 汪季涛, 甘德芳, 胡克玲. 不同贮藏温度对糙皮侧耳采后品质及木质素积累的影响[J]. 浙江农业学报, 2021, 33(2): 248-258.
[4]	崔鹏飞, 魏灵珠, 程建徽, 向江, 李明山, 吴江, . 不同砧木对天工翠玉葡萄生长和果实品质的影响[J]. 浙江农业学报, 2021, 33(1): 52-61.
[5]	廖朝美, 游敏芳, 谭光辉, 李杰章, 张依裕, 覃媛钰, 刘若余. 三穗鸭PRKCB基因内含子14的变异对蛋壳品质的影响[J]. 浙江农业学报, 2020, 32(9): 1574-1580.
[6]	李金武, 郁继华, 吕剑, 冯致, 杨海兴, 车旭升, 秦启杰, 张洋, 金宁. 不同覆盖方式对高原夏季露地松花菜产量、品质和土壤养分的影响[J]. 浙江农业学报, 2020, 32(9): 1626-1633.
[7]	喻宗岗, 蒋隽, 姚亚铃, 郭英, 李闯, 燕海峰. 雪峰乌骨鸡HSP70基因多态性与精液品质关联分析[J]. 浙江农业学报, 2020, 32(8): 1378-1384.
[8]	王同林, 叶红霞, 郑积荣, 李明. 番茄果实中主要风味物质研究进展[J]. 浙江农业学报, 2020, 32(8): 1513-1522.
[9]	顾赛麒, 王苏宁, 鲍嵘斌, 胡彬超, 杨晓霞, 张继磊, 陈景滢, 林招永, 丁玉庭, 柯志刚. 食品改良剂对丁香鱼干品质特性的影响[J]. 浙江农业学报, 2020, 32(7): 1263-1273.
[10]	韩立杰, 董伟欣, 张月辰. 不同水肥处理对小麦冠层结构、产量和籽粒品质的影响[J]. 浙江农业学报, 2020, 32(6): 953-962.
[11]	邓倩, 王羊, 邓群仙, 辛亚宁, 李雷, 龙星雨, 祝进, 张慧芬, 夏惠, 梁东. 蜀脆枣果实发育规律及品质积累特性分析[J]. 浙江农业学报, 2020, 32(4): 644-652.
[12]	王长进, 徐运林, 程昕昕, 周毅, 余海兵. 甜玉米种子营养品质主要性状全基因组关联分析[J]. 浙江农业学报, 2020, 32(3): 383-389.
[13]	裘劼人, 柴伟国, 童建新, 周历萍, 王淑珍. 质谱蛋白质组学研究中草莓雌蕊蛋白提取方法优化[J]. 浙江农业学报, 2020, 32(12): 2186-2191.
[14]	柯福艳, 徐知渊, 占金荣. 农产品质量安全消费者满意评价影响因素分析——来自浙江的调查[J]. 浙江农业学报, 2020, 32(12): 2271-2281.
[15]	马小华, 俞浙萍, 郑锡良, 胡晓金, 张淑文, 戚行江, 马靖艳. 靖州杨梅引种试验与表型聚类分析[J]. 浙江农业学报, 2020, 32(11): 1987-1993.