Dynamics of 5 fungicides residue in grape brewing fermentation process

doi:10.3969/j.issn.1004-1524.2019.01.19

›› 2019, Vol. 31 ›› Issue (1): 149-154.DOI: 10.3969/j.issn.1004-1524.2019.01.19

• Food Science • Previous Articles Next Articles

Dynamics of 5 fungicides residue in grape brewing fermentation process

ZHANG Lijun^1,2, ZHANG Hu², XU Mingfei², LIN Chunmian¹, WU Huizhen³, XU Jie², QIAN Mingrong^2,*

1. College of Environment, Zhejiang University of Technology, Hangzhou 310032, China;
2. Institute of Quality and Standard for Agro-Products, Zhejiang Academy of Agricultural Sciences, Hangzhou 310021, China;
3. College of Biology and Environmental Engineering, Zhejiang Shuren University, Hangzhou 310015, China

Received:2018-03-01 Online:2019-01-25 Published:2019-04-09

Abstract

Abstract: The residue of five fungicides (myclobutanil, famoxadone, mandipropamid, propiconazole, difenoconazole) in homemade wine fermentation process was analyzed by high performance liquid chromatography-mass spectrometry/mass spectrometry (HPLC-MS/MS). The effect of adding yeast on fungicides residue was also studied. It was shown that the average recoveries of the determination method ranged in 75.4%-112.5%. Five fungicides showed different degrees of degradation in the first fermentation stage, yet myclobutanil and mandipropamid showed no significant degradation during the fermentation process with yeast addition. The five fungicides residue showed a balanced state during the secondary fermentation stage. Adding yeast during fermentation did not significantly affect the degradation tendency. The residue of five fungicides in grape brewing process was not only related to the brewing process, but also related to the physicochemical properties of the fungicides.

Key words: fungicide, wine, pesticide residue

CLC Number:

ZHANG Lijun, ZHANG Hu, XU Mingfei, LIN Chunmian, WU Huizhen, XU Jie, QIAN Mingrong. Dynamics of 5 fungicides residue in grape brewing fermentation process[J]. , 2019, 31(1): 149-154.

References

[1] 李培培, 陈敏, 王军. QuEChERS-高效液相色谱法检测红葡萄酒中多菌灵和甲霜灵杀菌剂残留[J]. 食品与发酵工业, 2015, 41(1): 202-206.
LI P P, CHEN M, WANG J.Determination of carbendazim and metalaxyl pesticides in red wine by QuEChERS-high performance liquid chromatography[J]. Food and Fermentation Industries, 2015, 41(1): 202-206. (in Chinese with English abstract)
[2] 薛洁, 张敬, 梁萌萌, 等. 葡萄酒中农药残留的调查研究[J]. 酿酒科技, 2014 (7): 4-8.
XUE J, ZHANG J, LIANG M M, et al.Research on residual pesticide in grape wine[J]. Liquor-Making Science & Technology, 2014 (7): 4-8. (in Chinese with English abstract)
[3] 柳菡, 张亚莲, 丁涛, 等. 高效液相色谱-四极杆/静电场轨道阱高分辨质谱用于葡萄酒中111种农药残留的定性筛查与定量分析[J]. 分析测试学报, 2014, 33(5): 489-498.
LIU H, ZHANG Y L, DING T, et al.Screening and quantification of 111 pesticide residues in wines by high performance liquid chromatography-quadrupole/electrostatic field orbitrap high-resolution mass spectrometry[J]. Journal of Instrumental Analysis, 2014, 33(5): 489-498. (in Chinese with English abstract)
[4] 吕梦莎, 林能镖, 梁玉英, 等. 高效液相色谱法同时测定葡萄酒中16种添加剂[J]. 食品科学, 2016, 37(8): 222-225.
LYU M S, LIN N B, LIANG Y Y, et al.Simultaneous determination of 16 additives in wine by high performance liquid chromatography[J]. Food Science, 2016, 37(8): 222-225. (in Chinese with English abstract)
[5] MARTÍNEZ G, MORALES A, MAESTRO A, et al. Determination of nine fungicides in grape and wine using QuEChERS extraction and LC/MS/MS analysis[J]. Journal of AOAC International, 2015, 98(6): 1745-1751.
[6] 刘家涛. 脉冲电场降解红葡萄酒醪有机磷农药残留的研究[D]. 晋中: 山西农业大学, 2015.
LIU J T.The research of degradation on organophophorus pesticide residues in red wine mass processed by pulse electric fied[D]. Jinzhong: Shanxi Agricultural University,2015.(in Chinese with English abstract)
[7] CABRAS P, ANGIONI A.Pesticide residues in grapes, wine, and their processing products[J]. Journal of Agricultural and Food Chemistry, 2000, 48(4): 967-973.
[8] BELLINCONTRO A, PROSPERI P, DE SANTIS D, et al.Control of environmental parameters in postharvest partial dehydration of wine grapes reduces water stress[J]. Postharvest Biology and Technology, 2017, 134: 11-16.
[9] DEED R C, FEDRIZZI B, GARDNER R C.Influence of fermentation temperature, yeast strain, and grape juice on the aroma chemistry and sensory profile of Sauvignon Blanc wines[J]. Journal of Agricultural and Food Chemistry, 2017, 65(40): 8902-8912.
[10] BELLINCONTRO A, MATARESE F, D'ONOFRIO C, et al. Management of postharvest grape withering to optimise the aroma of the final wine: a case study on Amarone[J]. Food Chemistry, 2016, 213: 378-387.
[11] ?UŠ F, ?ESNIK H B, BOLTA Š V, et al. Pesticide residues in grapes and during vinification process[J]. Food Control, 2010, 21(11): 1512-1518.
[12] GARAU V L, DE MELO ABREU S, CABONI P, et al. Residue-free wines: fate of some quinone outside inhibitor (QoI) fungicides in the winemaking process[J]. Journal of Agricultural and Food Chemistry, 2009, 57(6): 2329-2333.
[13] VAQUERO-FERNÁNDEZ L, SANZ-ASENSIO J, FERNÁNDEZ-ZURBANO P, et al.Determination of fungicide pyrimethanil in grapes, must, fermenting must and wine[J]. Journal of the Science of Food and Agriculture, 2013, 93(8): 1960-1966.
[14] 高学峰, 杨继红, 王华. 葡萄及葡萄酒生产过程中副产物的综合利用研究进展[J]. 食品科学, 2015, 36(7): 289-295.
GAO X F, YANG J H, WANG H.Comprehensive utilization of by-products from grape and wine production[J]. Food Science, 2015, 36(7): 289-295. (in Chinese with English abstract)
[15] 王玉路, 王宗义, 贾昌喜, 等. 葡萄酒酿造过程中12种残留杀菌剂的归趋追踪[J]. 食品与发酵工业, 2016, 42(3): 114-118.
WANG Y L, WANG Z Y, JIA C X, et al.Fate tracing for 12 residual fungicides in grapes during vinification process[J]. Food and Fermentation Industries, 2016, 42(3): 114-118. (in Chinese with English abstract)

Dynamics of 5 fungicides residue in grape brewing fermentation process

RichHTML

PDF (PC)

Knowledge

Abstract

Cite this article

share this article

References

Related Articles 15

Recommended Articles

Metrics

Comments

[1]	XU Xuefen, NI Chunhui, LI Huixia, LI Huanyu, LI Wenhao, CHEN Yuan, HU Fangdi. Pathogen identification and indoor toxicity tests on root rot of Codonopsis pilosula [J]. Acta Agriculturae Zhejiangensis, 2021, 33(1): 96-103.
[2]	WANG Di, DI Shanshan, WANG Xinquan, ZHANG Changpeng, WANG Xiangyun, WANG Meng. Degradation of carbosulfan after its application in different growth stage of cowpea [J]. , 2020, 32(11): 2050-2058.
[3]	HUANG Jie, GONG Yongping, WEN Jifeng, YANG Rui, REN Lu, YAN Qigui. Expression of classical swine fever virus E2 protein in outer membrane vesicles of Escherichia coli and evaluation of its immunogenicity [J]. , 2018, 30(9): 1460-1466.
[4]	FANG Qi, ZHANG Jun, ZHOU Jinyun. Effect of processing on carbendazim residue in canned citrus [J]. , 2018, 30(9): 1599-1603.
[5]	YU Youyi, YANG Lu, LIAO Xiang, CHENG Ping, WU Shengli, LI Hong. Residual degradation dynamics of lambda-cyhalothrin and cypermethrin in apple and its removal method [J]. , 2018, 30(8): 1376-1381.
[6]	XIE Yunye, ZENG Sijin, YUAN Yue, WANG Lianping, FANG Li, WANG Hanrong. Pathogen identification and susceptibility to fungicides on tea anthracnose in Xinchang of Zhejiang Province [J]. , 2018, 30(7): 1188-1193.
[7]	GE Jing, JIANG Jinhua, CAI Leiming. Study on toxicity of three kinds of triazole fungicides on zebrafish (Danio rerio) [J]. , 2018, 30(5): 744-755.
[8]	LI Zhen, SUN Caixia, DAI Fen, ZHENG Weiran, YU Guoguang, YAO Jiarong, WANG Qiang. New requirements for grapes of national food safety standard GB 2763-2016 [J]. , 2018, 30(5): 840-847.
[9]	WANG Zongpei, WANG Shenyue, JIANG Junbao, LU Lei. Monitor and analysis on immune status of major infectious diseases of livestock and poultry in Ninghai County from 2013 to 2016 [J]. , 2018, 30(4): 554-559.
[10]	CHENG Pengfei, WANG Yan, YANG Qiyong, LIU Defu, LIU Tianzhong. Purification effect for swine wastewater with attached culture of microalgae [J]. , 2017, 29(9): 1564-1569.
[11]	REN Meishen1，2， WANG Yin1，2，*， YANG Zexiao1， YAO Xueping1， WU Xulong1，2， XIAO Lu1，2. Isolation， identification and biological characteristics analysis of Streptococcus parauberis [J]. , 2016, 28(5): 758-.
[12]	LIN Xingyu1，2， HU Ling1， WANG Yin1，2，*， YANG Zexiao1， YAO Xueping1， XIAOLu1， REN Meishen1， ZENG Xiangjie1. Isolation， identification and capsule serotyping of Pasteurella multocida originated from swine [J]. , 2016, 28(4): 558-.
[13]	XIE Daoyan， YANG Zhenguo， ZHOU Chuntao， CHAI Jianping， DA Aisi， NI Jing， JIANG Xiujun， LUO Yanjie*. Safety evaluation of new fungicide fluxapyroxadpyraclostrobin to mulberry and silkworm [J]. , 2016, 28(4): 654-.
[14]	DUAN Hai-ming, YU Li, HUANG Wei-dong, YU Hai-bing. Screening of high efficient fungicide for the pathogen of tomato gray mold and research on novel mixed agent [J]. , 2016, 28(12): 2060-2067.
[15]	RONG Qian， DAI Peng\\|fei， DENG Lin， QIN Hong\\|xia， LI Ying\\|lun*. Effects of twenty\\|five traditional antipyretic and antidote medicine extracts against Helicobacter pylori from swine in vitro [J]. , 2016, 28(1): 38-.