Acta Agriculturae Zhejiangensis ›› 2020, Vol. 32 ›› Issue (12): 2211-2217.DOI: 10.3969/j.issn.1004-1524.2020.12.12

• Quality and Safety of Agriculturel Products • Previous Articles     Next Articles

Deposition and residue of acetamiprid under protected celery cultivation

YU Xinru(), HE Hongmei, WANG Xiangyun, LI Yanjie, XU Lingying, ZHAO Xueping, ZHANG Changpeng*()   

  1. State Key Laboratory for Managing Biotic and Chemical Threats to the Quality and Safety of Agro-Products (in Prepared), Key Laboratory for Pesticide Residue Detection, Ministry of Agriculture and Rural Affairs, Institute of Quality and Standard for Agro-Products, Zhejiang Academy of Agricultural Sciences, Hangzhou 310021, China
  • Received:2020-05-14 Online:2020-12-25 Published:2020-12-25
  • Contact: ZHANG Changpeng

Abstract:

Based on the field experiments and laboratory tests, the deposition and residue characteristics of acetamiprid in celery under protected cultivation were studied, and a detection method was also established. The acetamiprid in soil and plant samples was extracted by using acetonitrile, purified by QuEChERs and detected by liquid chromagraphy-mass spectrometry. The average recoveries of acetamiprid in celery leaf, stem, root and soil were 100.2%-102.5%, 83.9%-93.5%, 97.0%-100.1% and 90.8%-94.4%, respectively. The amount of acetamiprid deposition decreased as celery leaf>soil>celery stem>celery root. The degradation curve of acetamiprid in celery leaf was in accordance with the first-order kinetic equation, and the degradation half-life of acetamiprid was 4.2-19.4 d. Seven days after application of acetamiprid with dosage of 18, 27 g·hm-2, the residues of acetamiprid in celery leaf and stem were 0.330 0-2.570 0, 0.004 7-0.030 0 mg·kg-1, respectively, which were below the maximum residue limit (3 mg·kg-1) of the Chinese national standard GB 2763—2019. The results could provide scientific reference for the rational use of acetamiprid on celery under protected cultivation.

Key words: acetamiprid, protected cultivation, residue, deposition, celery

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