质构技术快速辨别蜂蜜品种的研究

doi:10.3969/j.issn.1004-1524.2022.05.22

浙江农业学报 ›› 2022, Vol. 34 ›› Issue (5): 1073-1080.DOI: 10.3969/j.issn.1004-1524.2022.05.22

质构技术快速辨别蜂蜜品种的研究

窦文卿(), 柴春祥(), 刘玥, 鲁晓翔

天津商业大学生物技术与食品科学学院,天津市食品生物技术重点实验室,天津 300134

收稿日期:2020-11-07 出版日期:2022-05-25 发布日期:2022-06-06
作者简介:* 柴春祥,E-mail: ccxiang@tjcu.edu.cn
窦文卿(1997—),女,天津人,硕士研究生,研究方向为食品加工与贮藏。E-mail: dwqing_1@163.com
通讯作者: 柴春祥
基金资助:
天津市农业科技成果转化与推广项目(201901090);食品工程原理(19JKJS01058)

Rapid identification of different varieties of honey by its texture

DOU Wengqing(), CHAI Chunxiang(), LIU Yue, LU Xiaoxiang

Tianjin Key Laboratory of Food Biotechnology, College of Biotechnology and Food Science, Tianjin University of Commerce, Tanjin 300134, China

Received:2020-11-07 Online:2022-05-25 Published:2022-06-06
Contact: CHAI Chunxiang

摘要/Abstract

摘要：

为快速辨别不同品种蜂蜜,以枸杞蜂蜜、洋槐蜂蜜和紫云英蜂蜜为原料,本文推导了蜂蜜质构特性的测量原理,测定了不同蜂蜜的质构特性,分析了它们的质构特征。质构仪测定不同品种蜂蜜质构特征时,其探头受到的剪切力随测试时间、探头压缩距离的变化而变化。本文分析了质构仪探头受到的剪切力随测试时间、探头压缩距离的变化规律,获得不同蜂蜜的质构特性,进而辨别了蜂蜜的品种。结果表明:洋槐蜂蜜、紫云英蜂蜜、枸杞蜂蜜的质构特征值分别为8.01、5.96、5.34 Pa·s,组间方差分析显著,表明3种蜂蜜的质构特征值有显著性差异。对3种蜂蜜的测试数据(探头受到的剪切力随测试时间的变化关系)进行了回归分析,回归方程式符合蜂蜜质构特性的测量原理,决定系数(R²)均大于0.9,利用质构特性测试技术可以快速准确地区分3种蜂蜜。

关键词: 蜂蜜, 品种, 质构, 力学特性, 黏稠度

Abstract:

In order to quickly identify the different varieties of honey, the surveying principle of the honey texture was derived, the texture of different varieties of honey were tested and analyzed by using texture testing technique, and Chinese wolfberry honey, acacia honey and Chinese milk vetch honey were used as raw materials in this paper. When the texture of different varieties of honey was measured, the shear force on the probe changed with the change of test time and the distance of the probe. The variation of shear force on the probe with the test time and the moving distance of the probe were analyzed, and the texture characteristics of different honey were obtained, and then the varieties of honey were identified. The results showed that the texture characteristic values of acacia honey, Chinese milk vetch honey and Chinese wolfberry honey were 8.01, 5.96 and 5.34 Pa·s, respectively. The analysis of variance showed that there were significant differences among the texture characteristic values of the three kinds of honey. Regression analysis of the test data of the three kinds of honey showed that the coefficient of determination (R²) was all greater than 0.9, the regression equation was accordant to the surveying principle of the honey texture. Texture detection technology can be used to quickly and accurately distinguish three kinds of honey.

Key words: honey, variety, texture, mechanical properties, stickiness

中图分类号:

TS201.7

窦文卿, 柴春祥, 刘玥, 鲁晓翔. 质构技术快速辨别蜂蜜品种的研究[J]. 浙江农业学报, 2022, 34(5): 1073-1080.

DOU Wengqing, CHAI Chunxiang, LIU Yue, LU Xiaoxiang. Rapid identification of different varieties of honey by its texture[J]. Acta Agriculturae Zhejiangensis, 2022, 34(5): 1073-1080.

图/表 6

图1 质构仪压缩蜂蜜示意图 r1为质构仪探头外半径,r2为测量杯内半径。

Fig.1 Schematic diagram of honey compression by texture analyzer r1 is the outer radius of the probe of the texture detector,r2 is the inner radius of the measuring cup.

图2 质构仪探头受到的剪切力随测试时间的变化

Fig.2 The relationship between the shear force on the probe and the testing time

表1 不同品种蜂蜜对探头力的作用

Table 1 Effect of different varieties of honey on probe force

蜂蜜 Honey	F/N	变异系数 Coefficient of variation/%
洋槐蜂蜜	0.439±0.000 3 a	0.07
Acacia honey
紫云英蜂蜜	0.256±0.002 3 b	0.90
Chinese milk vetch honey
枸杞蜂蜜	0.223±0.006 5 c	2.91
Chinese wolfberry honey

图3 质构仪探头受到的剪切力随压缩距离的变化

Fig.3 The relationship between the shear force on the probe and the compression distance

图4 探头压缩枸杞蜂蜜受到的剪切力与测试时间的关系

Fig.4 The relationship between the shear force and the testing time of Chinese wolfberry honey

表2 探头受到的剪切力与测试时间的回归方程

Table 2 Regression equation of shear force on probe and testing time

蜂蜜 Honey	回归方程 Equation of regression	μ/(Pa·s)	R²
洋槐蜂蜜 Acacia honey	F= $8.01 × 10 ﹣ 2 t, t ≤ 5 0.44, t > 5$	8.01	0.994 6
紫云英蜂蜜 Chinese milk vetch honey	F= $5.96 × 10 ﹣ 2 t, t ≤ 5 0.26, t > 5$	5.96	0.977 3
枸杞蜂蜜 Chinese wolfberry honey	F= $5.34 × 10 ﹣ 2 t, t ≤ 5 0.22, t > 5$	5.34	0.968 7

表2 探头受到的剪切力与测试时间的回归方程

Table 2 Regression equation of shear force on probe and testing time

蜂蜜 Honey	回归方程 Equation of regression	μ/(Pa·s)	R²
洋槐蜂蜜 Acacia honey	F= $8.01 × 10 ﹣ 2 t, t ≤ 5 0.44, t > 5$	8.01	0.994 6
紫云英蜂蜜 Chinese milk vetch honey	F= $5.96 × 10 ﹣ 2 t, t ≤ 5 0.26, t > 5$	5.96	0.977 3
枸杞蜂蜜 Chinese wolfberry honey	F= $5.34 × 10 ﹣ 2 t, t ≤ 5 0.22, t > 5$	5.34	0.968 7

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质构技术快速辨别蜂蜜品种的研究

Rapid identification of different varieties of honey by its texture

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