Deposition and residue of acetamiprid under protected celery cultivation

doi:10.3969/j.issn.1004-1524.2020.12.12

Acta Agriculturae Zhejiangensis ›› 2020, Vol. 32 ›› Issue (12): 2211-2217.DOI: 10.3969/j.issn.1004-1524.2020.12.12

• Quality and Safety of Agriculturel Products • Previous Articles Next Articles

Deposition and residue of acetamiprid under protected celery cultivation

YU Xinru(), HE Hongmei, WANG Xiangyun, LI Yanjie, XU Lingying, ZHAO Xueping, ZHANG Changpeng^*()

State Key Laboratory for Managing Biotic and Chemical Threats to the Quality and Safety of Agro-Products (in Prepared), Key Laboratory for Pesticide Residue Detection, Ministry of Agriculture and Rural Affairs, Institute of Quality and Standard for Agro-Products, Zhejiang Academy of Agricultural Sciences, Hangzhou 310021, China

Received:2020-05-14 Online:2020-12-25 Published:2020-12-25
Contact: ZHANG Changpeng

Abstract

Abstract:

Based on the field experiments and laboratory tests, the deposition and residue characteristics of acetamiprid in celery under protected cultivation were studied, and a detection method was also established. The acetamiprid in soil and plant samples was extracted by using acetonitrile, purified by QuEChERs and detected by liquid chromagraphy-mass spectrometry. The average recoveries of acetamiprid in celery leaf, stem, root and soil were 100.2%-102.5%, 83.9%-93.5%, 97.0%-100.1% and 90.8%-94.4%, respectively. The amount of acetamiprid deposition decreased as celery leaf>soil>celery stem>celery root. The degradation curve of acetamiprid in celery leaf was in accordance with the first-order kinetic equation, and the degradation half-life of acetamiprid was 4.2-19.4 d. Seven days after application of acetamiprid with dosage of 18, 27 g·hm^-2, the residues of acetamiprid in celery leaf and stem were 0.330 0-2.570 0, 0.004 7-0.030 0 mg·kg^-1, respectively, which were below the maximum residue limit (3 mg·kg^-1) of the Chinese national standard GB 2763—2019. The results could provide scientific reference for the rational use of acetamiprid on celery under protected cultivation.

Key words: acetamiprid, protected cultivation, residue, deposition, celery

CLC Number:

S481⁺.8

YU Xinru, HE Hongmei, WANG Xiangyun, LI Yanjie, XU Lingying, ZHAO Xueping, ZHANG Changpeng. Deposition and residue of acetamiprid under protected celery cultivation[J]. Acta Agriculturae Zhejiangensis, 2020, 32(12): 2211-2217.

Figures/Tables 5

References 25

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样品 Sample	添加水平 Spike level/(mg·kg^-1)	回收率Recovery/%						平均回收率 Average recovery/%	相对标准偏差 RSD/%
样品 Sample	添加水平 Spike level/(mg·kg^-1)	1	2	3	4	5	6	平均回收率 Average recovery/%	相对标准偏差 RSD/%
芹菜叶	0.05	107.2	104.2	99.2	95.2	98.0	104.7	101.4	4.6
Celery leaf	0.10	101.4	100.4	107.5	105.2	93.8	93.1	100.2	5.8
	1.00	103.5	112.0	97.1	98.8	93.3	110.4	102.5	7.3
芹菜茎	0.05	81.1	81.2	83.8	87.3	81.9	88.3	83.9	3.7
Celery stem	0.10	82.2	89.6	95.7	87.9	105.0	100.7	93.5	9.1
	1.00	87.2	96.2	92.8	92.5	90.2	99.2	93.0	4.6
芹菜根	0.05	106.5	98.2	93.6	94.5	93.5	98.3	97.4	5.0
Celery root	0.10	101.5	100.5	96.3	100.5	100.6	101.3	100.1	1.9
	1.00	99.7	96.9	98.8	90.4	94.8	101.4	97.0	4.1
土壤Soil	0.02	85.4	89.6	92.9	103.8	89.4	90.7	92.0	6.8
	0.20	81.2	80.6	94.9	97.2	96.3	94.7	90.8	8.5
	1.00	86.0	96.3	96.8	95.4	102.5	89.2	94.4	6.2

样品 Sample	添加水平 Spike level/(mg·kg^-1)	回收率Recovery/%						平均回收率 Average recovery/%	相对标准偏差 RSD/%
样品 Sample	添加水平 Spike level/(mg·kg^-1)	1	2	3	4	5	6	平均回收率 Average recovery/%	相对标准偏差 RSD/%
芹菜叶	0.05	107.2	104.2	99.2	95.2	98.0	104.7	101.4	4.6
Celery leaf	0.10	101.4	100.4	107.5	105.2	93.8	93.1	100.2	5.8
	1.00	103.5	112.0	97.1	98.8	93.3	110.4	102.5	7.3
芹菜茎	0.05	81.1	81.2	83.8	87.3	81.9	88.3	83.9	3.7
Celery stem	0.10	82.2	89.6	95.7	87.9	105.0	100.7	93.5	9.1
	1.00	87.2	96.2	92.8	92.5	90.2	99.2	93.0	4.6
芹菜根	0.05	106.5	98.2	93.6	94.5	93.5	98.3	97.4	5.0
Celery root	0.10	101.5	100.5	96.3	100.5	100.6	101.3	100.1	1.9
	1.00	99.7	96.9	98.8	90.4	94.8	101.4	97.0	4.1
土壤Soil	0.02	85.4	89.6	92.9	103.8	89.4	90.7	92.0	6.8
	0.20	81.2	80.6	94.9	97.2	96.3	94.7	90.8	8.5
	1.00	86.0	96.3	96.8	95.4	102.5	89.2	94.4	6.2

试验点 Location	剂量 Dose/(g·hm^-2)	t	芹菜叶 Celery leaf	芹菜茎 Celery stem	芹菜根 Celery root	土壤 Soil
Zhejiang	27	2 h	2.840 0±0.250 0	0.120 0±0.016 0	0.028 0±0.013 0	0.003 5±0.000 2
		1 d	4.080 0±0.610 0	0.100 0±0.002 9	0.200 0±0.032 0	0.001 8±0.000 5
		3 d	4.110 0±0.420 0	0.110 0±0.016 0	0.160 0±0.031 0	—
		5 d	2.910 0±0.240 0	0.047 0±0.002 2	0.084 0±0.010 0	—
		7 d	2.570 0±0.420 0	0.030 0±0.002 1	0.031 0±0.006 4	—
		14 d	2.670 0±0.320 0	0.011 0±0.001 1	0.014 0±0.001 6	—
		21 d	1.890 0±0.230 0	0.006 8±0.001 7	0.009 4±0.001 4	—
	18	2 h	1.160 0±0.100 0	0.059 0±0.004 8	0.039 0±0.001 3	0.006 0±0.000 6
		1 d	1.890 0±0.310 0	0.072 0±0.012 0	0.067 0±0.005 9	0.000 6±0.000 1
		3 d	2.400 0±0.480 0	0.042 0±0.004 0	0.048 0±0.006 9	0.000 3±0.000 4
		5 d	1.580 0±0.210 0	0.017 0±0.001 4	0.017 0±0.000 2	—
		7 d	1.860 0±0.190 0	0.014 0±0.002 4	0.012 0±0.002 2	—
		14 d	1.110 0±0.210 0	0.002 0±0.000 1	0.004 5±0.000 1	—
		21 d	0.870 0±0.093 0	0.001 8±0.000 5	0.003 7±0.000 5	—
Shandong	27	2 h	1.790 0±0.200 0	0.046 0±0.009 0	0.061 0±0.003 1	0.000 5±0.000 1
		1 d	0.950 0±0.055 0	0.022 0±0.004 3	0.022 0±0.003 5	0.000 4±0.000 2
		3 d	0.680 0±0.078 0	0.016 0±0.005 7	0.009 2±0.000 6	—
		5 d	0.630 0±0.008 0	0.007 8±0.002 9	0.008 0±0.000 2	—
		7 d	0.420 0±0.068 0	0.004 7±0.000 3	0.005 3±0.000 2	—
		14 d	0.150 0±0.021 0	0.001 2±0.000 1	0.003 5±0.000 2	—
		21 d	0.039 0±0.018 0	0.000 6±0.000 1	0.001 7±0.000 2	—
	18	2 h	1.000 0±0.020 0	0.017 0±0.003 9	0.002 8±0.000 3	0.001 1±0.001 6
		1 d	0.520 0±0.057 0	0.013 0±0.003 4	0.007 5±0.000 9	—
		3 d	0.400 0±0.045 0	0.004 7±0.001 4	0.005 9±0.001 3	—
		5 d	0.590 0±0.073 0	0.005 3±0.000 7	0.003 6±0.000 5	—
		7 d	0.330 0±0.091 0	0.004 7±0.000 8	0.003 5±0.000 9	—
		14 d	0.100 0±0.008 0	0.001 3±0.000 4	0.002 8±0.000 6	—
		21 d	0.210 0±0.081 0	0.000 9±0.000 1	0.001 7±0.000 3	—

试验点 Location	剂量 Dose/(g·hm^-2)	t	芹菜叶 Celery leaf	芹菜茎 Celery stem	芹菜根 Celery root	土壤 Soil
Zhejiang	27	2 h	2.840 0±0.250 0	0.120 0±0.016 0	0.028 0±0.013 0	0.003 5±0.000 2
		1 d	4.080 0±0.610 0	0.100 0±0.002 9	0.200 0±0.032 0	0.001 8±0.000 5
		3 d	4.110 0±0.420 0	0.110 0±0.016 0	0.160 0±0.031 0	—
		5 d	2.910 0±0.240 0	0.047 0±0.002 2	0.084 0±0.010 0	—
		7 d	2.570 0±0.420 0	0.030 0±0.002 1	0.031 0±0.006 4	—
		14 d	2.670 0±0.320 0	0.011 0±0.001 1	0.014 0±0.001 6	—
		21 d	1.890 0±0.230 0	0.006 8±0.001 7	0.009 4±0.001 4	—
	18	2 h	1.160 0±0.100 0	0.059 0±0.004 8	0.039 0±0.001 3	0.006 0±0.000 6
		1 d	1.890 0±0.310 0	0.072 0±0.012 0	0.067 0±0.005 9	0.000 6±0.000 1
		3 d	2.400 0±0.480 0	0.042 0±0.004 0	0.048 0±0.006 9	0.000 3±0.000 4
		5 d	1.580 0±0.210 0	0.017 0±0.001 4	0.017 0±0.000 2	—
		7 d	1.860 0±0.190 0	0.014 0±0.002 4	0.012 0±0.002 2	—
		14 d	1.110 0±0.210 0	0.002 0±0.000 1	0.004 5±0.000 1	—
		21 d	0.870 0±0.093 0	0.001 8±0.000 5	0.003 7±0.000 5	—
Shandong	27	2 h	1.790 0±0.200 0	0.046 0±0.009 0	0.061 0±0.003 1	0.000 5±0.000 1
		1 d	0.950 0±0.055 0	0.022 0±0.004 3	0.022 0±0.003 5	0.000 4±0.000 2
		3 d	0.680 0±0.078 0	0.016 0±0.005 7	0.009 2±0.000 6	—
		5 d	0.630 0±0.008 0	0.007 8±0.002 9	0.008 0±0.000 2	—
		7 d	0.420 0±0.068 0	0.004 7±0.000 3	0.005 3±0.000 2	—
		14 d	0.150 0±0.021 0	0.001 2±0.000 1	0.003 5±0.000 2	—
		21 d	0.039 0±0.018 0	0.000 6±0.000 1	0.001 7±0.000 2	—
	18	2 h	1.000 0±0.020 0	0.017 0±0.003 9	0.002 8±0.000 3	0.001 1±0.001 6
		1 d	0.520 0±0.057 0	0.013 0±0.003 4	0.007 5±0.000 9	—
		3 d	0.400 0±0.045 0	0.004 7±0.001 4	0.005 9±0.001 3	—
		5 d	0.590 0±0.073 0	0.005 3±0.000 7	0.003 6±0.000 5	—
		7 d	0.330 0±0.091 0	0.004 7±0.000 8	0.003 5±0.000 9	—
		14 d	0.100 0±0.008 0	0.001 3±0.000 4	0.002 8±0.000 6	—
		21 d	0.210 0±0.081 0	0.000 9±0.000 1	0.001 7±0.000 3	—

Deposition and residue of acetamiprid under protected celery cultivation

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